HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → N'-t-butyl-N-benzoyl-N'-(2-thiophenecarbonyl)hydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Thiophenecarbonyl chloride | HCID 78928 | — |
| Reactant | N'-tert-butylbenzohydrazide | HCID 299436 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N'-t-butyl-N-benzoyl-N'-(2-thiophenecarbonyl)hydrazine | HCID 15452002 | — |
Reaction Steps
N'-t-butyl-N-benzoylhydrazine (1.0 g) was dissolved in 20 ml toluene. 50% aqueous sodium hydroxide (1.25 g) was added followed by 2-thiophene-carbonylchloride (0.76 g). The mixture was stirred at room temperature for 14 hours. The solid product, N'-t-butyl-N-benzoyl-N'-(2-thiophenecarbonyl)hydrazine, was removed by filtration and washed with water. m.p. >200° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06013836 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-6985cd67d7c24b26ae4586520d9f0d6f |
| Source note | uspto-grants-2000_01 |