HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19365451, compound → 4-Amino-2-(2-ethylhexanoylamino)-phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19365451 | HCID 19365451 | — |
| Catalyst | HCID 178506447 | HCID 178506447 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Amino-2-(2-ethylhexanoylamino)-phenol | HCID 19365450 | — |
Reaction Steps
39 g of preliminary product 1 were hydrogenated with H2 /Raney nickel in 200 ml ethanol. The hydrogenation was conducted over a period of 2 hours and within a temperature range from 20 to 40 C. at a pressure of 2. 106Pa. The catalyst was filtered off under suction and 400 ml water were added. The dried, oily product (37 g) which was separated was reacted further without additional purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06015654 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-a5a347101d3b4423bfa31a74ff8dece9 |
| Source note | uspto-grants-2000_01 |