HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 19365867, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 4,5,6,7-Tetrahydrothieno(3,2-c)pyridine | HCID 3085076 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 19365867 | HCID 19365867 | — |
Reaction Steps
The product from Step 1 (9.57 g, 40 mmol) was dissolved in CHCl3 (150 mL) at 0° C. and treated with bromine (2.1 mL, 40 mmol) dropwise over 10 minutes. The mixture was stirred for 16 h at room temperature then filtered to afford the title compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06015817 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-23487d2a2ad94b66bfb21a72b64a3eb3 |
| Source note | uspto-grants-2000_01 |