HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzyl chloride → 2-(2-Chlorophenyl)-4'-iodoacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzyl chloride | HCID 11906 | — |
| Reactant | 4-Iodo-N-methoxy-N-methyl-benzamide | HCID 5461756 | — |
| Product | 2-(2-Chlorophenyl)-4'-iodoacetophenone | HCID 19365962 | — |
Reaction Steps
The title compound was prepared from α,2-dichlorotoluene and O,N-dimethyl-4-iodobenzenehydroxamic acid (see Preparation 30) by a similar method to that of Preparation 20(i) as a colourless solid, m.p. 105-106° C., which was characterised by 1H-N.M.R. spectroscopy.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06015825 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-42d71a100361488785799ceb606b0af6 |
| Source note | uspto-grants-2000_01 |