Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 850264Generated: October 30, 2026

Methyl nitrite → HCID 86583921, compound

https://huagongshe.com/reaction/850264

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl nitriteHCID 12231—
ReactantHCID 19362515HCID 19362515—
ProductHCID 86583921HCID 8658392158.1%

Reaction Steps

According to the method described under 1.1., 34.8 g (0.166 mol) of 3,4-bis(methylthio)benzyl cyanide are reacted with 0.166 mol methylnitrite. After the isolation 23.0 g (58%) α-hydroxyimino-3,4-bis(methylthio)benzyl cyanide are obtained as a brown substance with a melting point of 131-133° C. Elemental analysis: C10H10N2OS2 (238.33)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06017675
Source datasetuspto-grants-2000_01
ORD IDord-2ac8f4f664ff4c5882be8fe0ed743b7f
Source noteuspto-grants-2000_01