Thiophenol → HCID 178422816, compound

Participants

Reaction Steps

To a solution of 4-chloro-2-hydroxy-6-methyl-3-nitropyridine (188 mg, 1.0 mmol) in 2 mL of EtOH and 0.2 mL (1.4 mmol) of Et3N was added 0.11 mL (1.0 mmol) of PhSH. Precipitation occurred immediately and the solution was allowed to stir at room temperature for 16 h. The solid was filtered and washed with EtOH to afford II-2.

Provenance & Evidence