Acetyl chloride → HCID 178475066, compound

Participants

Reaction Steps

Compound 9 was prepared by the method described for the preparation of compound 7 from AC2 (1.2 mmol) and acetyl chloride (1.2 mmol), and isolated as a white powder (0.10 g): mp 111-116° C.; FAB-MS m/e 705 (MH+). Anal. calcd. for C37H49N8O5F·1.0 TFA·1.0 anisole·1.0 H2O (901.78): C, 57.54; H, 6.35; N, 12.43; KF, 2.0. Found: C, 57.71; H, 6.27; N, 12.49; KF, 2.32.

Provenance & Evidence