Benzene → HCID 54443004, compound

HRID 850920Notes

Reaction equation

HRID 850920 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][C:6]1([C:19]([NH2:21])=[O:20])[C:18]2[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=2[C:12]2[C:7]1=[CH:8][CH:9]=[CH:10][CH:11]=2.[CH:22]1[CH:27]=CC=C[CH:23]=1.CCCBr>C(N(CC)CC)C>[CH2:23]([NH:1][CH2:2][CH2:3][CH2:4][CH2:5][C:6]1([C:19]([NH2:21])=[O:20])[C:7]2[CH:8]=[CH:9][CH:10]=[CH:11][C:12]=2[C:13]2[C:18]1=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH2:22][CH3:27]

Participants

5

Reactant 3

HCID 241BenzeneHCID 78401-BromopropaneHCID 20456803HCID 20456803, compound

Product 1

HCID 54443004HCID 54443004, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

A solution of 9-(4-aminobutyl)-9-aminocarbonylfluorene in benzene containing one equivalent of n-propyl bromide and triethylamine is stirred for several hours. Removal of the reaction solvent and distillation of the product affords 9-(4-n-propylaminobutyl)-9-aminocarbonylfluorene.

Workup

  1. customRemoval of the reaction solvent and distillation of the product

Sources & evidence

ORD record
ord-51af9b071ed54cc2b9b079c4986d44e5
Source dataset
uspto-grants-1983_05
Patent number
US04382093

Reaction notes

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