HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → Ethyl 3-(3-methoxyphenyl)-1,2,5,6-tetrahydro-1-pyridine-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | 1-Benzyl-3-(3-methoxyphenyl)-1,2,5,6-tetrahydropyridine | HCID 15105450 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Ethyl 3-(3-methoxyphenyl)-1,2,5,6-tetrahydro-1-pyridine-carboxylate | HCID 20502638 | — |
Reaction Steps
A solution of 11.4 g of the product of Step B, 25 ml of benzene and 5.9 ml of ethyl chloroformate was refluxed for 3 hours and was then evaporated to dryness under reduced pressure. Excess ethyl chloroformate was entrained with benzene to obtain 11 g of ethyl 3-(3-methoxyphenyl)-1,2,5,6-tetrahydro-1-pyridine-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04382942 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-633c5a16566a4d199b0f7de5efb8980d |
| Source note | uspto-grants-1983_05 |