HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13139543, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86738862 | HCID 86738862 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13139543 | HCID 13139543 | — |
Reaction Steps
A suspension of zinc dust (5.18 g) in a solution of bis(N-allyloxycarbonyl-D-cystine bis-allyl ester (5.18 g) in methanol (50 ml) at 0° C. is stirred vigorously while adding concentrated hydrochloric acid (3.5 ml) in one portion. After two minutes, the mixture is worked up as in the above Preparation B to afford the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04382949 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-d5563e9fa2cd4ce2b75da9ea83bf2cbf |
| Source note | uspto-grants-1983_05 |