HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-1-[3-(trifluoromethyl)phenyl]ethan-1-ol → HCID 13079628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-1-[3-(trifluoromethyl)phenyl]ethan-1-ol | HCID 30514 | — |
| Reactant | HCID 20502759 | HCID 20502759 | — |
| Product | HCID 13079628 | HCID 13079628 | — |
Reaction Steps
The compound was prepared as in Example 4, from 1-[4-(11-hydroxyundecyloxy)phenyl]propan-2-one (7.3 g) and 2-hydroxy-2-(3-trifluoromethylphenyl)-ethanamine (4.7 g) and purified by chromatography on silica gel in 5% methanol dichloromethane, mp 45°-50° C. as a 50:50 mixture of diastereoisomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04382958 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-06657a6ddaf4432b9f6c1c1927385498 |
| Source note | uspto-grants-1983_05 |