HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isopropylphenol → HCID 13136917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isopropylphenol | HCID 12059 | — |
| Reactant | HCID 13381780 | HCID 13381780 | — |
| Product | HCID 13136917 | HCID 13136917 | 28.2% |
Reaction Steps
Prepared by the method described in Example 1 from 3-isopropylphenol (150 g, 0.66 moles) and 4-oxo-3-piperidinecarboxylate hydrochloride (114 g, 0.59 moles). Recrystallization from dilute aqueous hydrochloric acid yielded the product (46.6 g) as the hydrochloride, mp 257°-261° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04382939 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-2828774bd0554344afccda221dcf135d |
| Source note | uspto-grants-1983_05 |