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HRID851193

反应详情

EQUATION

反应方程式

HRID 851193 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)c1cccc(O)c1
HCID11450

3-tert-Butylphenol

C10H14O

结构：COC(=O)C1CNCCC1=O.Cl
HCID2724028

Methyl 4-oxopiperidine-3-carboxylate--hydrogen chloride (1/1)

C7H12ClNO3

PRODUCTS

生成物

1
结构：CC(C)(C)c1ccc2c3c(c(=O)oc2c1)CNCC3
HCID13136921

未命名化合物

收率 57.1%

PROCEDURE

实验过程

Prepared by the method described for Example 1 from 3-t-butylphenol (15 g, 0.1 moles) and methyl 4-oxo-3-piperidinecarboxylate hydrochloride (19.3 g, 0.1 moles). Recrystallization from ethyl acetate gave the product (14.7 g), mp 181°-186° C.

WORKUP

后处理

  1. customPrepared by the method
  2. customRecrystallization from ethyl acetate