HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetone → HCID 13136936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetone | HCID 6571 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 13136924 | HCID 13136924 | — |
| Product | HCID 13136936 | HCID 13136936 | 35.6% |
Reaction Steps
Prepared by the method described for example 26 from 1,2,3,4-tetrahydro-8-methyl-9-nitro-5H-[1]benzopyrano[3,4-c]pyridin-5-one (2.0 g, 0.008 moles), triethylamine (2.3 ml, 0.017 moles), and 1-chloro-2-propanone (0.7 g, 0.008 moles). Recrystallization from methanol gave the product (0.9 g), mp 166°-168° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04382939 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-1322b18f4a2b418a9a54a3ba6e2bcffe |
| Source note | uspto-grants-1983_05 |