HRID851206

反应详情

EQUATION

反应方程式

HRID 851206 的结构方程式

PROCEDURE

实验过程

Prepared by the method described for Example 26 from 1,2,3,4-tetrahydro-8-methoxy-9-nitro-5H-[1]benzopyrano[3,4-c]pyridin-5-one (5.52 g, 0.02 moles) and 1-chloro-2-propanone (3.5 g, 0.038 moles). Recrystallization from methanol gave the product (5.7 g), mp 222°-225° C.

WORKUP

后处理

  1. customPrepared by the method
  2. customRecrystallization from methanol