HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 851509Generated: November 2, 2026
HCID 20430894, compound → HCID 53844146, compound
https://huagongshe.com/reaction/851509
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 20430894 | HCID 20430894 | — |
| Reactant | HCID 178526132 | HCID 178526132 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | HCID 53844146 | HCID 53844146 | 51.6% |
Reaction Steps
A mixture of 3,3-dimethyl-1-cyclopentene-1-carboxylic acid (2 g) and thio-benzoic acid (2.37 g) is heated to 120° C. for 14 hours under Argon stream. The reaction mixture is cooled, taken up with a small amount of cyclohexane and filtered yielding 2.05 g of trans 2-benzoylthio-3,3-dimethylcyclopentyl carboxylic acid. M.p. 131° C. (from hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04385062 |
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| Source dataset | uspto-grants-1983_05 |
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| ORD ID | ord-902c74537d8d490f818a74c20674e96e |
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| Source note | uspto-grants-1983_05 |
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