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HRID851554

反应详情

EQUATION

反应方程式

HRID 851554 的结构方程式

REACTANTS

反应物

3
结构：BrC(Br)Br
HCID5558

Bromoform

CHBr3

结构：O=C(Cl)CCl
HCID6577

Chloroacetyl chloride

C2H2Cl2O

结构：Cl.NOC(c1ccccc1)c1ccccc1
HCID198859

Hydroxylamine, O-(diphenylmethyl)-, hydrochloride

C13H14ClNO

PRODUCTS

生成物

1
结构：O=C(CCl)NOC(c1ccccc1)c1ccccc1
HCID12774346

未命名化合物

收率 86%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

This compound was prepared from diphenylmethoxyamine hydrochloride and chloroacetyl chloride by the method described in Preparation 1; m.p. 115°-117° νmax (CHBr3) include 3400 (NH), 1692 cm-1 (CO-N), τ(DMSO d6) 0.55 (NH), 2.60 (Ph) 4.01 (CHPh2), 6.02 (CH2). Yield 86%.

WORKUP

后处理

  1. customdescribed in Preparation 1