HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoform → Diphenylmethyl Chloroacetohydroxamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoform | HCID 5558 | — |
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | Hydroxylamine, O-(diphenylmethyl)-, hydrochloride | HCID 198859 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | Diphenylmethyl Chloroacetohydroxamate | HCID 12774346 | 86% |
Reaction Steps
This compound was prepared from diphenylmethoxyamine hydrochloride and chloroacetyl chloride by the method described in Preparation 1; m.p. 115°-117° νmax (CHBr3) include 3400 (NH), 1692 cm-1 (CO-N), τ(DMSO d6) 0.55 (NH), 2.60 (Ph) 4.01 (CHPh2), 6.02 (CH2). Yield 86%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04385177 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-ba2224fdb34f4ba7a22f3dd312a5e526 |
| Source note | uspto-grants-1983_05 |