HRID851561

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID679

Dimethyl sulfoxide

C2H6OS

HCID702

Ethanol

C2H6O

HCID9250

Cyclobutane

C4H8

$结构：COC(=O)/C(=N\OC1(OC(=O)OC(C)(C)C)CCC1)c1ccco1$

HCID20501519

未命名化合物

PRODUCTS

生成物

$结构：COC(=O)/C(=N\OC1(C(=O)O)CCC1)c1ccco1$

HCID12774350

未命名化合物

收率 94%

PROCEDURE

实验过程

This compound was prepared from methyl Z-2-(1-tert-butyloxycarbonyloxycyclobutyloxyimino)-2-(fur-2-yl)acetate as described in Preparation 7(b), m.p. 133°-134°. λmax (EtOH) 284 nm (ε15,900), νmax (Nujol) 3500-2100 (bonded OH), 1750 (CO2H), 1708 cm-1 (α,β-unsaturated --CO2R), τ(DMSO d6) 7.2-8.5 (cyclobutane), 2.1, 3.12, 3.33 (furyl), 6.09 (--CO2CH3). Yield 94%