HRID851566

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6365179

O-Phenylhydroxylamine hydrochloride

C6H8ClNO

$结构：COC(=O)/C(=N\OC1(C(=O)O)CCCC1)c1ccco1$

HCID88736760

未命名化合物

PRODUCTS

生成物

$结构：COC(=O)/C(=N\OC1(C(=O)NOc2ccccc2)CCCC1)c1ccco1$

HCID20501531

未命名化合物

收率 44%

PROCEDURE

实验过程

This compound prepared from methyl Z-2-(carboxycyclopent-1-yloxyimino)-2-(fur-2-yl)acetate and phenoxyamine hydrochloride as described in Preparation 7(c), was purified by chromatography on silica gel plates in ethyl acetate-light petroleum b.p. 40°-60° (3:1 v/v). τ(DMSO d6) 2.5-3.1 (phenyl), 7.7-8.1, 8.1-8.5 (cyclopentyl), 2.0, 3.28, 3.02 (furyl), 6.03 (methyl). Yield 44%

WORKUP

后处理

customwas purified by chromatography on silica gel plates in ethyl acetate-light petroleum b.p. 40°-60° (3:1 v/v)