HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 54074435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 4,4'-Dichlorobenzanilide | HCID 237478 | — |
| Reactant | Methyl 8-bromooctanoate | HCID 11107373 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54074435 | HCID 54074435 | — |
Reaction Steps
As described in example 1(a), 2.4 g (0.1 mol) of sodium hydride, 25.2 g (0.1 mol) of 4-chloro-N-(4-chlorophenyl)-benzamid, 200 ml dimethylformamide, 23.7 g (0.1 mol) of 8-bromocaprylic acid methyl ester and 3 g (0.02 mol) of sodium iodide are reacted. Reaction time: 5.5 hours; reaction temperature: 110° C. The crude product is used in the next step without any further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04386031 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-ecb6df33830e49f998c07e16388c2ae8 |
| Source note | uspto-grants-1983_05 |