HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 54385324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Fluorobenzoyl chloride | HCID 67879 | — |
| Reactant | 8-(4-Methoxyphenylamino)-caprylic acid methyl ester | HCID 13025814 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54385324 | HCID 54385324 | — |
Reaction Steps
As described in example 3(b), the reaction is carried out with 5.6 g (20 mmol) of 8-(4-methoxyphenylamino)-caprylic acid methyl ester, 5 g (50 mmol) of triethylamine, 150 cc. of toluene and 4 g (25 mmol) of 4-fluorobenzoic acid chloride. Reaction time: 5 hours, reaction temperature: 25° C. The crude product is used in the next reaction step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04386031 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-95c3342db8e0489a82a233324c991fa8 |
| Source note | uspto-grants-1983_05 |