HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethyl phosphite → Phosphinecarboxylic acid, dimethoxy-, butyl ester, oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethyl phosphite | HCID 8472 | — |
| Reactant | Butyl chloroformate | HCID 61140 | — |
| Product | Phosphinecarboxylic acid, dimethoxy-, butyl ester, oxide | HCID 512108 | — |
Reaction Steps
From 10.0 ml (85 mmole) of trimethylphosphite and 8.7 g (64 mmole) of n-butyl chloroformate. (100° C., 1.5 hours). Yield 10.9 g (81%). Bp1.0 97°-100° C. nD25 1,4269.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04386081 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-ba4cc6d1032a4712a11df0aa739d8dbf |
| Source note | uspto-grants-1983_05 |