HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl chloroformate → Phosphinecarboxylic acid, dimethoxy-, 1-methylethyl ester, oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl chloroformate | HCID 7917 | — |
| Reactant | Trimethyl phosphite | HCID 8472 | — |
| Product | Phosphinecarboxylic acid, dimethoxy-, 1-methylethyl ester, oxide | HCID 512107 | — |
Reaction Steps
From 10.0 ml (85 mmole) of trimethylphosphite and 7.8 g (64 mmole) of i-propyl chloroformate. (100° C., 2 hours). Yield 8.0 g (64%). Bp2 90°-2° C. nD25 1,4202.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04386081 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-9f7924b51e93442ebea3ff9b2f82267e |
| Source note | uspto-grants-1983_05 |