HRID851707

反应详情

EQUATION

反应方程式

HRID 851707 的结构方程式

PROCEDURE

实验过程

From 26.6 g (0.10 mole) of tri-n-butylphosphite and 18.9 g (0.20 mole) of methyl chloroformate (80° C., 6 hours). Yield 22.4 g (89%). Bp0.2 85°-105° C., nD25 1.4310.

WORKUP

后处理

  1. customBp0.2 85°-105° C.