HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → Phosphinecarboxylic acid, dibutoxy-, methyl ester, oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | Tributyl phosphite | HCID 7623 | — |
| Product | Phosphinecarboxylic acid, dibutoxy-, methyl ester, oxide | HCID 512112 | — |
Reaction Steps
From 26.6 g (0.10 mole) of tri-n-butylphosphite and 18.9 g (0.20 mole) of methyl chloroformate (80° C., 6 hours). Yield 22.4 g (89%). Bp0.2 85°-105° C., nD25 1.4310.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04386081 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-5f8b0f5f9b444cd283681712aa0fc796 |
| Source note | uspto-grants-1983_05 |