Trimethyl phosphite → HCID 13753784, compound

HRID 851709Notes

Reaction equation

HRID 851709 reaction equation
C[O:2][P:3]([O:6][CH3:7])[O:4][CH3:5].Cl[C:9]([O:11][CH2:12][CH3:13])=[O:10]>>[CH2:12]([O:11][C:9]([P:3](=[O:2])([O:6][CH3:7])[O:4][CH3:5])=[O:10])[CH3:13]

Participants

3

Reactant 2

HCID 8472Trimethyl phosphiteHCID 10928Ethyl chloroformate

Product 1

HCID 13753784HCID 13753784, compound

Procedure

From 10,0 ml (85 mmole) of trimethylphosphite and 10.0 ml (105 mmole) of ethyl chloroformate (100° C., 1,5 hours). Yield 12,5 g (80%). Bp15 122° C.

Workup

  1. customBp15 122° C.

Sources & evidence

ORD record
ord-7e1d2280e496468e9e0071c10e100b57
Source dataset
uspto-grants-1983_05
Patent number
US04386081

Reaction notes

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