HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Sulfite → 2-(Butylsulfonyl)cyclopentanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Sulfite | HCID 24437 | — |
| Reactant | Monoperoxyphthalic acid | HCID 75329 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-(Butylsulfonyl)cyclopentanone | HCID 289555 | — |
Reaction Steps
2-Buthylthiocyclopentanone (88 g) was reacted with a 30% excess solution of mono-perphthalic acid in ether at 0° C. After the reaction was completed, the excess mono-perphthalic acid was treated with sodium sulfite, and the resultant solution was washed, evaporated to remove the solvent, and then distilled, thereby giving 2-butylsulfonylcyclopentanone (78 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07252849B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-e82c9b732d564f92a08e72aaa22da92b |
| Source note | uspto-grants-2007_08 |