HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 14905832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | HCID 17785308 | HCID 17785308 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 14905832 | HCID 14905832 | 91% |
Reaction Steps
6-Amino-1-neopentyluracil (90c) (5.9 g, 0.03 mol) were dissolved in 1 N NaOH (50 ml) and then under vigorous stirring dimethylsulfate (3.9 ml, 0.033 mol) dropwise added at room temp. A precipitate separated and was collected after 2 hours. After washing with water and drying in a vacuum desiccator resulted 5.76 g (91%) of colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253176B1 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-8aa4f9e6d54a492da30669c00d4b7780 |
| Source note | uspto-grants-2007_08 |