HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 17906270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 17906318 | HCID 17906318 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 17906270 | HCID 17906270 | — |
Reaction Steps
The title compound is prepared from a mixture of 3[4-(2-bromo-ethoxy)-phenyl]-6-fluoro-benzo[d]isoxazole, pyrrolidine, potassium carbonate, potassium iodide and 5% aqueous acetonitrile at 75° C. essentially as described above in Example 13, except that the column is eluted with 10% methanol in ethyl acetate. Purity by LC/MS=99%, [M+H]+=327.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253165B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-37dac2efef8448fb92ee5bb3d9c6aea5 |
| Source note | uspto-grants-2007_08 |