HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 69419679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Aminoindan hydrochloride | HCID 122764 | — |
| Reactant | HCID 17906346 | HCID 17906346 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 69419679 | HCID 69419679 | — |
Reaction Steps
The title compound is prepared from a mixture of 3-[4-(3-bromo-propoxy)-phenyl]-6-fluoro-benzo[d]isoxazole, 2-aminoindan hydrochloride, potassium carbonate, potassium iodide and 4% aqueous acetonitrile essentially as described above in Example 13 except that 3.2 equivalents of potassium carbonate is used. Purity by LC/MS=93%, [M+H]+=403.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253165B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-ef60311cc5e04492816f8aa6fea79faf |
| Source note | uspto-grants-2007_08 |