HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 58928261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 17906346 | HCID 17906346 | — |
| Reactant | HCID 21218568 | HCID 21218568 | — |
| Product | HCID 58928261 | HCID 58928261 | — |
Reaction Steps
The title compound is prepared from a mixture of 3-[4-(3-bromo-propoxy)-phenyl]-6-fluoro-benzo[d]isoxazole, thiophen-3-yl-methylamine hydrochloride (Table No. 1, SM 1), potassium carbonate, potassium iodide and 4% aqueous acetonitrile essentially as described above in Example 13 except that 3.2 equivalents of potassium carbonate is used. Purity by LC/MS=95%, [M+H]+=383.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253165B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-bae6a17f34b74d4993e8bb756511feb2 |
| Source note | uspto-grants-2007_08 |