HRID85219

反应详情

EQUATION

反应方程式

HRID 85219 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

475 mg (1.65 mmol) of the compound from Example 36A are dissolved in 48 ml of THF. 50 mg (0.05 mmol) of palladium on carbon are then added, and the mixture is hydrogenated at RT in a hydrogen atmosphere under atmospheric pressure. The mixture is then filtered, the filter cake is washed three times with THF and the filtrate is freed from the solvent. The reaction product is reacted further without further purification.

WORKUP

后处理

  1. filtrationThe mixture is then filtered
  2. washthe filter cake is washed three times with THF
  3. customThe reaction product is reacted further without further purification