HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2,3,4-Tetrahydroisoquinoline → HCID 58928276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2,3,4-Tetrahydroisoquinoline | HCID 7046 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-[4-(3-Bromo-propoxy)-phenyl]-benzo[b]thiophene | HCID 17906314 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 58928276 | HCID 58928276 | — |
Reaction Steps
The title compound is prepared from 3-[4-(3-bromo-propoxy)-phenyl]-benzo[b]thiophene, 1,2,3,4-tetrahydroisoquinoline, potassium carbonate and acetonitrile essentially as described above in Example 118. Purity by LC/MS=94%, [M+H]+=400.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253165B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-c012ea1441514fd09482ece01fd112d6 |
| Source note | uspto-grants-2007_08 |