Piperidine → 2-(piperidin-1-ylsulfonyl)aniline

HRID 852232Notes

Reaction equation

HRID 852232 reaction equation
[NH:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[N+:7]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[S:16](Cl)(=[O:18])=[O:17])([O-])=O>>[N:1]1([S:16]([C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=2[NH2:7])(=[O:18])=[O:17])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 8082PiperidineHCID 155402-Nitrobenzenesulfonyl chloride

Product 1

HCID 11328162-(piperidin-1-ylsulfonyl)anilineYield 58%

Procedure

The title compound (0.59 g, 58%) was obtained as a brown solid from piperidine and 2-nitrobenzenesulfonylchloride following the same procedure as described in preparation 2.

Sources & evidence

ORD record
ord-3189dae6040541e9915a6a38aea97f8b
Source dataset
uspto-grants-2007_08
Patent number
US07253171B2

Reaction notes

Loading…