2-Pyridinecarboxaldehyde → HCID 9900083, compound

HRID 852326Notes

Reaction equation

HRID 852326 reaction equation
Cl[C:2]1[CH:3]=[C:4]([N:8]2[N:12]=[N:11][C:10]([C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=3)=[N:9]2)[CH:5]=[CH:6][CH:7]=1.[SH:19][C:20]1C=C(NC2C=CC=CC=2)C=CC=1.N1C=CC=CC=1C=O>>[CH3:20][S:19][C:2]1[CH:3]=[C:4]([N:8]2[N:12]=[N:11][C:10]([C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=3)=[N:9]2)[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 3

HCID 142732-PyridinecarboxaldehydeHCID 99213692-[2-(3-chlorophenyl)-2H-tetrazol-5-yl]pyridineHCID 66941026HCID 66941026, compound

Product 1

HCID 9900083HCID 9900083, compound

Procedure

Following the procedure described in EXAMPLE 1 for the synthesis of 2-[2-(3-chlorophenyl)-2H-tetrazol-5-yl]pyridine, 3-mercaptophenylaniline (41.8 mg, 0.3 mmol) and 2-pyridinecarboxaldehyde (32.1 mg, 0.3 mmol) were employed to obtain 2-[2-(3-Methylmercaptophenyl)-2H-tetrazol-5-yl]pyridine as an orange solid.

Sources & evidence

ORD record
ord-3c0bf2cbe63241d8a22da6641e15e2ec
Source dataset
uspto-grants-2007_08
Patent number
US07253190B2

Reaction notes

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