1-Chloro-4-iodobenzene → HCID 69457682, compound

HRID 852380Notes

Reaction equation

HRID 852380 reaction equation
[CH2:1]([O:3][C:4](=[O:21])[C:5]([O:8][C:9]1[CH:14]=[CH:13][C:12]([O:15][CH2:16][CH2:17][C:18]#[CH:19])=[CH:11][C:10]=1[CH3:20])([CH3:7])[CH3:6])[CH3:2].[Cl:22][C:23]1[CH:28]=[CH:27][C:26](I)=[CH:25][CH:24]=1>>[CH2:1]([O:3][C:4](=[O:21])[C:5]([O:8][C:9]1[CH:14]=[CH:13][C:12]([O:15][CH2:16][CH2:17][C:18]#[C:19][C:26]2[CH:27]=[CH:28][C:23]([Cl:22])=[CH:24][CH:25]=2)=[CH:11][C:10]=1[CH3:20])([CH3:6])[CH3:7])[CH3:2]

Participants

3

Reactant 2

HCID 125101-Chloro-4-iodobenzeneHCID 86602541HCID 86602541, compound

Product 1

HCID 69457682HCID 69457682, compound

Procedure

In analogy to the procedure described in example 13B], 2-(4-but-3-ynyloxy-2-methyl-phenoxy)-2-methyl-propionic acid ethyl ester (example 16A]) and 1-chloro-4-iodo-benzene gave the title compound as a light yellow viscous oil.

Sources & evidence

ORD record
ord-00a3a570da9c4ccc9973d888f3eff0d4
Source dataset
uspto-grants-2007_08
Patent number
US07253192B2

Reaction notes

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