HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic acid 5-(4-trifluoromethoxy-phenyl)-pent-4-ynyl ester → HCID 69460308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic acid 5-(4-trifluoromethoxy-phenyl)-pent-4-ynyl ester | HCID 11616756 | — |
| Reactant | HCID 67402766 | HCID 67402766 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 69460308 | HCID 69460308 | — |
Reaction Steps
In analogy to the procedure described in. example 20A], 2-(2,5-dichloro-4-hydroxy-phenoxy)-2-methyl-propionic acid methyl ester was treated with methanesulfonic acid 5-(4-trifluoromethoxy-phenyl)-pent-4-ynyl ester (example 1G]) in acetonitrile at the reflux temperature of the solvent for 3 h to give the title compound as colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253192B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-9fb1bf3dc5c5434eb911069067f8fd9b |
| Source note | uspto-grants-2007_08 |