Sodium Iodide → HCID 69461161, compound

HRID 852423Notes

Reaction equation

HRID 852423 reaction equation
[CH3:1][Si:2]([CH3:16])([CH3:15])[C:3]#[C:4][CH2:5][C:6]1([CH2:9]OS(C)(=O)=O)[CH2:8][CH2:7]1.[Na+].[I-:18]>>[I:18][CH2:9][C:6]1([CH2:5][C:4]#[C:3][Si:2]([CH3:16])([CH3:15])[CH3:1])[CH2:8][CH2:7]1

Participants

3

Reactant 2

HCID 5238Sodium IodideHCID 86602547HCID 86602547, compound

Product 1

HCID 69461161HCID 69461161, compound

Procedure

In analogy to the procedure described in example 34G], methanesulfonic acid 1-(3-trimethylsilanyl-prop-2-ynyl)-cyclopropylmethyl ester and NaI gave after 30 min at reflux temperature the title compound as orange oil.

Workup

  1. customgave after 30 min

Sources & evidence

ORD record
ord-8eca8d99e3a446ec92efb706df52f56a
Source dataset
uspto-grants-2007_08
Patent number
US07253192B2

Reaction notes

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