1-(4-Methyl-3-pyridinyl)ethanone → 2-Bromo-1-(4-methylpyridin-3-yl)ethan-1-one hydrobromide

HRID 852436Notes

Reaction equation

HRID 852436 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][N:5]=[CH:4][C:3]=1[C:8](=[O:10])[CH3:9].[BrH:11].BrBr>>[BrH:11].[Br:11][CH2:9][C:8]([C:3]1[CH:4]=[N:5][CH:6]=[CH:7][C:2]=1[CH3:1])=[O:10]

Participants

3

Reactant 2

HCID 109424811-(4-Methyl-3-pyridinyl)ethanoneHCID 86584092HBr bromine

Product 1

HCID 227309902-Bromo-1-(4-methylpyridin-3-yl)ethan-1-one hydrobromideYield 85%

Procedure

The title compound was synthesised according to Example 4 1-(4-methyl-pyridin-3-yl)-ethanone and HBr/bromine in 85% yield as grey solid. MS (m/e): 214.0 (M+H, 100%).

Sources & evidence

ORD record
ord-5fb6b3c7424140028db7d32ac83bc078
Source dataset
uspto-grants-2007_08
Patent number
US07253197B2

Reaction notes

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