HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Methyl-3-pyridinyl)ethanone → 2-Bromo-1-(4-methylpyridin-3-yl)ethan-1-one hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Methyl-3-pyridinyl)ethanone | HCID 10942481 | — |
| Reactant | HBr bromine | HCID 86584092 | — |
| Product | 2-Bromo-1-(4-methylpyridin-3-yl)ethan-1-one hydrobromide | HCID 22730990 | 85% |
Reaction Steps
The title compound was synthesised according to Example 4 1-(4-methyl-pyridin-3-yl)-ethanone and HBr/bromine in 85% yield as grey solid. MS (m/e): 214.0 (M+H, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253197B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-5fb6b3c7424140028db7d32ac83bc078 |
| Source note | uspto-grants-2007_08 |