HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 72466434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 3-[(Aminothioxomethyl)amino]benzenesulfonamide | HCID 43148917 | — |
| Product | HCID 72466434 | HCID 72466434 | 82% |
Reaction Steps
A mixture of 2.3 g (9.9 mmol) 3-Thioureido-benzenesulfonamide and 17 ml N,N-Dimethylformamide dimethyl acetal was heated for 2 h to 90° C. The precipitate was filtered of washed with DCM/diethyl ether 1:3 and dried to yield 2.8 g (82%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253197B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-4452ed59d260418a942b5ff2ee2dd0e4 |
| Source note | uspto-grants-2007_08 |