HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → 1,1-Dimethylethyl {1,1-dimethyl-2-[(phenylmethyl)oxy]ethyl}carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | Methanesulfonic acid 2-tert-butoxycarbonylamino-2-methyl-propyl ester | HCID 11659022 | — |
| Reactant | 1,1-Dimethylethyl [1,1-dimethyl-2-(phenyloxy)ethyl]carbamate | HCID 86602880 | — |
| Product | 1,1-Dimethylethyl {1,1-dimethyl-2-[(phenylmethyl)oxy]ethyl}carbamate | HCID 57718559 | — |
Reaction Steps
1,1-Dimethylethyl {1,1-dimethyl-2-[(phenylmethyl)oxy]ethyl}carbamate (D275) was prepared from 2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2-methylpropyl methanesulfonate (D273) in an analogous manner to 1,1-dimethylethyl [1,1-dimethyl-2-(phenyloxy)ethyl]carbamate (D274) using phenylmethanol instead of phenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253198B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-ce868e6eef6b4c588cfdbe61caaf4f38 |
| Source note | uspto-grants-2007_08 |