Dimethylformamide → HCID 66621956, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of 444-methoxy-phenyl)-pyrimidine-2-thiol (225a) (1.00 g, 4.58 mmol) in DMF (30 mL) was added 4-bromomethyl-benzoic acid methyl ester (1.05 g, 4.58 mmol). The mixture was heated at 60° C. for 1 h and evaporated to dryness to form the compound 226a, which was used in the next without purification. LRMS=366.4(calc.), 367.4 (found).

Provenance & Evidence