化工社化工社 化学情報印刷レポート · 研究参考用
Water → Perfluorooctanoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Octanoyl fluoride, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro- | HCID 67634 | — |
| 生成物 | Perfluorooctanoic acid | HCID 9554 | — |
反応手順
A 250 ml PFA vessel equipped with a stirrer was used. Water (100 g, 5.6 mol) was temperature conditioned to 60° C. within the vessel, following which C7F15COF (50 g, 0.120 mol; prepared by the method described in JP-A 8-231462) having a purity of 99.9 wt % was added dropwise under stirring in an attempt to form C7F15COOH by a hydrolysis reaction. However, a gel formed, which made stirring impossible.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07253315B2 |
| 出典データセット | uspto-grants-2007_08 |
| ORD ID | ord-ac8e42cdc53a4f5d8e452e14a54cd255 |
| 出典メモ | uspto-grants-2007_08 |