HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 69039384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(Bromomethyl)benzonitrile | HCID 86996 | — |
| Reactant | HCID 69037912 | HCID 69037912 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 69039384 | HCID 69039384 | — |
Reaction Steps
In analogy to the procedure described in Example 3b), the alkylation of (RS)-2-(4-hydroxy-phenoxy)-N-methyl-butyramide with 4-bromomethyl-benzonitrile in 2-butanone using potassium carbonate as the base yielded the (RS)-2-[4-(4-cyano-benzyloxy)-phenoxy]-N-methyl-butyramide as a white solid; MS: m/e=325 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253318B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-bdcd0a9508df4cb8bd339336be8024f9 |
| Source note | uspto-grants-2007_08 |