HCID 86603207, compound → HCID 86603206, compound

Participants

Reaction Steps

1,3-[di(tert-butoxycarbonylamino)]-2-tetradecylthioacetylthiopropane (example 15d) (0.300 g, 0.52 mmol) was dissolved in ether saturated in gaseous hydrochloric acid (55 ml). The mixture was stirred at room temperature. After 96 hours of reaction, the precipitate which formed was filtered, washed several times with diethyl ether and dried to give the desired compound in the form of a white powder.

Provenance & Evidence