Aluminium lithium hydride → HCID 22935657, compound

Participants

Reaction Steps

11-Ethyl-7-methylspiro[5,5]undec-8-en-1-one was reduced with LiAlH4 according to the general procedure (example 2, procedure 3) to give the title compound in 92% yield, as a 4:1 mixture of isomers. The crude product was purified by bulb-to-bulb distillation (B.p.=102° C./0.03 mbar).

Provenance & Evidence