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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 853743Generated: October 30, 2026

HCID 12093578, compound → HCID 22935667, compound

https://huagongshe.com/reaction/853743

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 12093578HCID 12093578—
ReactantHCID 12093579HCID 12093579—
ReactantHCID 178418348HCID 178418348—
ProductHCID 22935667HCID 2293566743%

Reaction Steps

A mixture of 7-methylspiro[4,5]decan-1-one and 8-methylspiro[4,5]decan-1-one and methyl lithium were reacted together according to the general procedure (example 2, procedure 5) to give the title compound in 43% yield. The crude product was purified by column chromatography on silicagel (eluent: cyclohexane/ethyl acetate 29:1) and bulb-to-bulb distillation (B.p.=68° C./0.04 mbar).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07256170B2
Source datasetuspto-grants-2007_08
ORD IDord-d9c64de3f329484bb64c036a063a8bdc
Source noteuspto-grants-2007_08