HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxybenzaldehyde → HCID 69516964, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxybenzaldehyde | HCID 101 | — |
| Reactant | HCID 58932670 | HCID 58932670 | — |
| Product | HCID 69516964 | HCID 69516964 | — |
Reaction Steps
The title compound was obtained as an off-white solid (38.5 mg, 18.2%) from compound 1C and 3-hydroxybenzaldehyde in the same manner as that used in the preparation of Example 1 by acidifying the aqueous washings and recrystallization of the crude product from MeOH. LC/MS m/z 356 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07256208B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-34d89c5378634a68a915d813cab87d79 |
| Source note | uspto-grants-2007_08 |